In Structural Studies Department of CMMS PAS we focus our attention on recognizing and understanding structure of organic molecules, drugs, small peptides and proteins. Main analytical technique which we are using is solid-state NMR spectroscopy.
Structural characterization of new matters represents a key challenge for researchers dealing with scientific disciplines such as organic and bioorganic chemistry, polymer chemistry as well as new materials engineering. Understanding the properties of substances and knowledge of their three-dimensional structure are essential in accounting for the relationship between morphology and functions. There are a number of experimental techniques that are dedicated to the study of structures. The NMR spectroscopy and mass spectrometry are leading analytical techniques developed in our Laboratory;
The main field of interest is the application of the NMR spectroscopy and mass spectrometry in the structure analysis of organic, bioorganic compounds and polymers. The synthetic materials and natural products are investigated both in liquid and solid phases. The correlation between the molecular and/or supermolecular structure and physico-chemical properties is one of the leading projects.
Solid State NMR spectroscopy is used as a tool to search the polymorphism and pseudopolymorphism phenomenon, analysis of intra- and intermolecular contacts e.g. strong and weak hydrogen bonding, aromatic-aromatic interactions, molecular packing effects. The influence of intermolecular interactions on NMR shielding parameters is investigated by means of experimental and theoretical methods.
The methodology of measurements that allow understanding the mechanism of the phase transition on the molecular level is developed. The mode of phase reorientation is searched in the complementary approach employing DSC (Differential Scanning Calorimetry) and variable temperature high resolution Solid State NMR.
Subtle structural features, e.g., deviation from perfect periodicity (static distortion), have influence on the physical properties of the solid state. Most solid materials contain some level of disorder. It is not always possible to investigate the local distortion of structure by means of XRD methods, which reflect long range order. Solid State NMR spectroscopy, representing the local electronic environment for each nucleus correlated with XRD of powdered materials is employed for detailed analysis of materials and thermal processes.
Developing the methodology of measurements of peptides interactions with lipid bilayers is one of the newest projects. Opioid peptides are studied by means of the HR MAS approach.
2022
Miksa B. The Phenazine Scaffold used as Cytotoxic Pharmacophore Applied in Bactericidal, Antiparasitic and Antitumor Agents. Helv. Chim. Acta 2022, 105, e202200066 link
Chotera-Ouda A., Jeziorna A., Kazmierski S., Dolot R., Dudek M. K., Potrzebowski M. J. „Crystal memory” affects the properties of peptide hydrogels – the case of the cyclic Tyr-Tyr dipeptide. Chem. Eur. J. 2022, 28, e202202005 link
Pawlak T., Paluch P., Dolot R., Bujacz G., Potrzebowski M. J. New salts of teriflunomide (TFM) – Single crystal X-ray and solid state NMR investigation. Solid State Nucl. Magn. Reson. 2022, 122, 101820 link
Marín-Villa P., Arauzo A., Drużbicki K., Fernandez-Alonso F. Unraveling the Ordered Phase of the Quintessential Hybrid Perovskite MAPbI3─Thermophysics to the Rescue. J. Phys. Chem. Lett. 2022, 13, 8422–8428 link
Le Marchand T., Schubeis T., Bonaccorsi M., Paluch P., Lalli D., Pell A. J., Andreas L. B., Jaudzems K., Stanek J., Pintacuda G. 1H-Detected Biomolecular NMR under Fast Magic-Angle Spinning. Chem. Rev. 2022, 122, 9943–10018 link
Raval P., Dhennin M., Vezin H., Pawlak T., Roussel P., Nguyen T.-Q., Reddy G. N. M. Understanding the p-doping of spiroOMeTAD by tris(pentafluorophenyl)borane. Electrochim. Acta 2022, 424, 140602 link
Patyra A., Dudek M. K., Kiss A. K. LC-DAD–ESI-MS/MS and NMR Analysis of Conifer Wood Specialized Metabolites. Cells 2022, 11, 3332 link
Raval P., Trébosc J., Pawlak T., Nishiyama Y., Brown S. P., Reddy G. N. M. Combining heteronuclear correlation NMR with spin-diffusion to detect relayed Cl–H–H and N–H–H proximities in molecular solids. Solid State Nucl. Magn. Reson. 2022, 120, 101808 link
Herc A. S., Dudek M. K., Kaźmierski S., Bojda J., Kaczorowski W., Januszewicz B., Kowalewska A. Spontaneous formation of hierarchical structures in some polylactide/polysilsesquioxane blends. CrystEngComm 2022, 24, 7465-7481 link
Khalaji M., Paluch P., Potrzebowski M. J., Dudek M. K. Narrowing down the conformational space with solid-state NMR in crystal structure prediction of linezolid cocrystals. Solid State Nucl. Magn. Reson. 2022, 121, 101813 link
Ziental D., Zając J., Lewandowski K., Dlugaszewska J., Potrzebowski M. J., Sobotta L. Oxospirochlorins as new promising photosensitizers against priority pathogens. Dyes Pigm. 2022, 201, 110240 link
Paluch P., Augustyniak R., Org M.-L., Vanatalu K., Kaldma A., Samoson A., Stanek J. NMR Assignment of Methyl Groups in Immobilized Proteins Using Multiple-Bond 13C Homonuclear Transfers, Proton Detection, and Very Fast MAS. Front. Mol. Biosci. 2022, 9, 828785 link
Michalak P., Paluch P., Guńka P. A. Crystal Structure and Energetics of Arsenic(III)-Oxide Intercalates with Rubidium Chloride and Their Comparison with Isostructural Intercalates of Potassium Halides. Cryst. Growth Des. 2022, 22, 711-717 link
Gobis K., Szczesio M., Olczak A., Pawlak T., Augustynowicz-Kopeć E., Krause M., Główka M. L. Relationship between the Crystal Structure and Tuberculostatic Activity of Some 2-Amidinothiosemicarbazone Derivatives of Pyridine. Materials 2022, 15, 349 link
Pawlak T., Oszajca M., Szczesio M., Potrzebowski M. J. Solid-State Study of the Structure, Dynamics, and Thermal Processes of Safinamide Mesylate─A New Generation Drug for the Treatment of Neurodegenerative Diseases. Mol. Pharmaceutics 2022, 19, 287–302 link
Luginbuhl B. R., Raval P., Pawlak T., Du Z., Wang T., Kupgan G., Schopp N., Chae S., Yoon S., Yi A., Jung Kim H., Coropceanu V., Brédas J.-L., Nguyen T.-Q., Reddy G. N. M. Resolving Atomic-Scale Interactions in Nonfullerene Acceptor Organic Solar Cells with Solid-State NMR Spectroscopy, Crystallographic Modelling, and Molecular Dynamics Simulations. Adv. Mater. 2022, 34, 2105943 link
Dudek M. K., Drużbicki K. Along the road to crystal structure prediction (CSP) of pharmaceutical-like molecules. CrystEngComm 2022, 24, 1665-1678 link
Gleńsk M., Dudek M. K., Kinkade P., Santos E. C. S., Glinski V. B., Ferreira D., Seweryn E., Kaźmierski S., Calixto J. B., Glinski J. A. Isolation of Echimidine and Its C-7 Isomers from Echium plantagineum L. and Their Hepatotoxic Effect on Rat Hepatocytes. Molecules 2022, 27, 2869 link
Potrzebowska N., Cavani O., Kazmierski S., Wegrowe J.-E., Potrzebowski M. J., Clochard M.-C. Molecular dynamics between amorphous and crystalline phases of e-b eam irradiate d piezoelectric PVDF thin films employing solid-state NMR spectroscopy. Polym. Degrad. Stab. 2022, 195, 109786 link
2021
Pawlak T., Szczesio M., Potrzebowski M. J. Single-Crystal X-ray and Solid-State NMR Characterisation of AND-1184 and Its Hydrochloride Form. Materials 2021, 14, 7175 link
Lalik E., Drużbicki K., Irvine G., Gutmann M., Rudić S., Manuel P., Petříček V., Krzystyniak M. Interplay between Local Structure and Nuclear Dynamics in Tungstic Acid: A Neutron Scattering Study. J. Phys. Chem. C 2021, 125, 23864–23879 link
Domański M. A., Kraszewski K., Paluch P., Guńka P. A. Arsenic(III)-oxide Intercalates with Potassium Chloride: Water-Induced Varieties and New Synthesis Methods. Cryst. Growth Des. 2021, 9, 5215–5222 link
Vazquez-Fernandez I., Druzbicki K., Fernandez-Alonso F., Mukhopadhyay S., Nockemann P., Parker S., Rudic S., Stana S-M., Tomkinson J., Yeadon D., Seddon K., Plechkova N. Spectroscopic Signatures of Hydrogen-bonding Motifs in Protonic Ionic-Liquid Systems: Insights from Diethylammonium Nitrate in the Solid State. J. Phys. Chem. C 2021, 125, 24463-24476 link
Czylkowska A., Szczesio M., Raducka A., Rogalewicz B., Kręcisz P., Czarnecka K., Szymański P., Pitucha M., Pawlak T. Cytotoxic Activity against A549 Human Lung Cancer Cells and ADMET Analysis of New Pyrazole Derivatives. Int. J. Mol. Sci. 2021, 22, 6692. link
Trzeciak K., Chotera-Ouda A., Bak-Sypien I., Potrzebowski M. J. Mesoporous Silica Particles as Drug Delivery Systems-The State of the Art in Loading Methods and the Recent Progress in Analytical Techniques for Monitoring These Processes. Pharmaceutics 2021, 13, 950 link
Dudek M. K., Kazmierski S., Potrzebowski M. J. Editor Webb G. A. Fast and very fast MAS solid state NMR studies of pharmaceuticals. Annual Rep. NMR Spectrosc. 2021, 103, 97-189. link
Wroblewska A., Lauriol G., Mloston G., Bantreil X., Lamaty F. Expedient synthesis of N-Oxy-Heterocyclic Carbenes (NOHC) ligands and metal complexes using mechanochemistry. J. Organomet. Chem. 2021, 949, 121914 link
Blauz A., Rychlik B., Plazuk D., Peccati F., Jimenez-Oses G. Steinke U., Sierant M., Trzeciak K., Skorupska E., Miksa B. Biotin-phenosafranin as a new photosensitive conjugate for targeted therapy and imaging. New J. Chem. 2021, 45, 9691-9702 link
Koźmiński P., Gawęda W., Rzewuska M., Kopatys A., Kujda S., Dudek M. K., Halik P. K., Królicki L., Gniazdowska E. Physicochemical and Biological Study of 99mTc and 68Ga Radiolabelled Ciprofloxacin and Evaluation of [99mTc]Tc-CIP as Potential Diagnostic Radiopharmaceutical for Diabetic Foot Syndrome Imaging. Tomography 2021, 7, 829-842 link
Bieszczad B., Garbicz D., Switalska M., Dudek M. K., Warszycki D., Wietrzyk J., Grzesiuk E., Mieczkowski A. Improved HDAC Inhibition, Stronger Cytotoxic Effect and Higher Selectivity against Leukemias and Lymphomas of Novel, Tricyclic Vorinostat Analogues. Pharmaceuticals 2021, 14, 851 link
Miksa B., Steinke U., Trzeciak K., Sniechowska J., Rozanski A. Thermostable Fluorescent Capsules with the Cross-Linked Heterocyclic Polymer Shell from Poly(pyrrole-phenosafranin). Macromol. Chem. Phys. 2021, 222, 2000396 link
Gleńsk M., Dudek M. K., Rybacka A., Włodarczyk M., Fecka I. Triterpenoids from strawberry Fragaria × ananassa Duch. cultivar Senga Sengana leaves. Ind. Crops Prod. 2021, 169, 113668 (1-8) link
Pawlak T., Sudgen I., Bujacz G., Iuga D., Brown S. P., Potrzebowski M. J. Synergy of Solid-State NMR, Single-Crystal X-ray Diffraction, and Crystal Structure Prediction Methods: A Case Study of Teriflunomide (TFM). Cryst. Growth Des. 2021, 21, 3328–3343 link
Trzeciak K., Kaźmierski S., Drużbicki K, Potrzebowski M. J. Mapping of Guest Localization in Mesoporous Silica Particles by Solid-State NMR and Ab Initio Modeling: New Insights into Benzoic Acid and p-Fluorobenzoic Acid Embedded in MCM-41 via Ball Milling. J. Phys. Chem. C 2021, 125, 10096–10109 link
Dudek M.K., Kaźmierski S, Potrzebowski M.J. Fast and Very Fast MAS Solid State NMR Studies of Pharmaceuticals. Annual Rep. NMR Spectrosc. 2021 link
Dahlman, C.J., Kennard, R.M., Paluch, P., Venkatesan, N.R., Chabinyc, M.L., Manjunatha Reddy, G.N. Dynamic Motion of Organic Spacer Cations in Ruddlesden-Popper Lead Iodide Perovskites Probed by Solid-State NMR Spectroscopy. Chem. Mater. 2021, 33, 642-656 link
Khalaji M., Potrzebowski M. J., Dudek M. K. Virtual Cocrystal Screening Methods as Tools to Understand the Formation of Pharmaceutical Cocrystals—A Case Study of Linezolid, a Wide-Range Antibacterial Drug. Cryst. Growth Des. 2021, 21, 2301–2314 link
Gleńsk M., Dudek M.K., Ciach M., Włodarczyk M. Isolation and structural determination of flavan-3-ol derivatives from the Polypodium vulgare L. rhizomes water extract. Nat. Prod. Res. 2021, 35, 1474–1483 link
2020
Trzeciak K., Kaźmierski S., Wielgus E., Potrzebowski M. J. DiSupLo – New extremely easy and efficient method for loading of active pharmaceutical ingredients into the pores of MCM-41 mesoporous silica particles. Microporous Mesoporous Mater. 2020, 308, 110506 link
Khalaji M., Wróblewska A., Wielgus E., Bujacz G. D., Dudek M. K., Potrzebowski M. J. Structural variety of heterosynthons in linezolid cocrystals with modified thermal properties. Acta Cryst. 2020, B76, 892–912 link
Dudek M. K., Śniechowska J., Wróblewska A., Kaźmierski S., Potrzebowski M. J. Cocrystals “divorce and marriage”: when a binary system meets an active multifunctional synthon in a ball mill. Chem. Eur. J. 2020, 26, 13264-13273 link
Dudek M. K., Paluch P., Śniechowska J., Nartowski K. P., Day G. M., Potrzebowski M. J. Crystal structure determination of an elusive methanol solvate – hydrate of catechin using crystal structure prediction and NMR crystallography. CrystEngComm 2020, 22, 4969-4981 link
Bieszczad B., Garbicz D., Trzybiński D., Dudek M. K., Woźniak K., Grzesiuk E., Mieczkowski A. Unsymmetrically-Substituted 5,12-dihydrodibenzo[b,f][1,4]diazocine-6,11-dione Scaffold – A Useful Tool for Bioactive Molecules Design. Molecules 2020, 25, 2855 (1-24) link
Pawłowska K. A., Hałasa R., Dudek M. K., Majdan M., Jankowska K., Granica S. Antibacterial and anti-inflammatory activity of bistort (Bistorta officinalis) aqueous extract and its major components. Justification of the usage of the medicinal plant material as a traditional topical agent. J. Ethnopharmacol. 2020, 260, 113077 link
Dudek M. K., Paluch P., Pindelska E. Crystal structures of two furazidin polymorphs revealed by a joint effort of crystal structure prediction and NMR crystallography. Acta Cryst. 2020, B76, 322-335 link
Wróblewska A., Śniechowska J., Kaźmierski S., Wielgus E., Bujacz G.D., Mlostoń G., Chworos A., Suwara J., Potrzebowski M.J. Application of 1-hydroxy-4,5-dimethyl-imidazole 3-oxide as coformer in formation of pharmaceutical cocrystals. Pharmaceutics 2020, 12, 359 (1-22) link
Pawlak T., Czajkowska-Szczykowska D., Jastrzebska I., Santillan R., Seroka B., Maj J., Morzycki J.W., Labra-Vázquez P., Farfán N., Bujacz G.D., Potrzebowski M.J. Influence of hydrogen/fluorine substitution on structure, thermal phase transitions, and internal molecular motion of aromatic residues in the crystal lattice of steroidal rotors. Cryst. Growth Des. 2020, 20, 2202-2216 link
Jędrzejewska H., Wielgus E., Kaźmierski S., Rogala H., Wierzbicki M., Wróblewska A., Pawlak T., Potrzebowski M.J., Szumna A. Porous molecular capsules as non‐polymeric transducers of mechanic forces to mechanophores. Chem. Eur. J. 2019, accepted for publication 2019 link
Trzeciak K., Paluch P., Pawlak T., Różański A., Dudek M.K., Potrzebowski M.J. The influence of the stereochemistry and C-end chemical modification of dermorphin derivatives on the peptide-phospholipid interactions. Biochim. Biophys. Acta, Biomembranes 1862, 2020, 183066 link
Gleńsk M., Dudek M.K., Ciach M., Włodarczyk M. Isolation and structural determination of flavan-3-ol derivatives from the Polypodium vulgare L. rhizomes water extract. Nat. Prod. Res. 2020, accepted for publication link
2019
Gliński J.A., Proudfoot J., Madura I., Zhang H., Gleńsk M., Day V., Dudek M.K. Spontaneous Stereoselective Oxidation of Crystalline Avermectin B1a to its C-8a-(S)-Hydroperoxide. J. Nat. Prod. 2019, 82, 3477−3481 link
Dudek M.K., Wielgus E., Paluch P., Śniechowska J., Kostrzewa M., Day G.M., Bujacz G.D., Potrzebowski M.J. Understanding the formation of apremilast cocrystals. Acta Cryst. B75, 2019, 803-814 link
Kołacińska K., DeVol T.A., Seliman A.F., Bliznyuk V.N., Dudek J., Dudek M.K., Piotrowski P., Trojanowicz M. Application of new covalently-bound diglycolamide sorbent in sequential injection analysis flow system for sample pretreatment in ICP-MS determination of 239Pu at ppt level. Talanta 205, 2019, 120099 link
Jacek P., Kubiak K., Ryngajłło M., Rytczak P., Paluch P., Bielecki S. Modification of bacterial nanocellulose properties through mutation of motility related genes in Komagataeibacter hansenii ATCC 53582. N. Biotechnol. 52, 2019, 60-68 link
Rankin, A.G.M., Trébosc, J., Paluch, P., Lafon, O., Amoureux, J.-P. Evaluation of excitation schemes for indirect detection of 14N via solid-state HMQC NMR experiments.J. Magn. Reson. 2019, 303, 28-41 linkPaluch, P., Rankin, A.G.M., Trébosc, J., Lafon, O., Amoureux, J.-P.Analysis of HMQC experiments applied to a spin ½ nucleus subject to very large CSA. Solid State Nucl. Magn. Reson. 2019, 100, 11-25 link
Dudek, M.K., Day, G.M. Explaining crystallization preferences of two polyphenolic diastereoisomers by crystal structure prediction. CrystEngComm 2019, 21, 2067-2079 link
Rozga-Wijas, K., Sierant, M., Wielgus, E., Miksa, B.J. Polyhedral octasilsesquioxanes labelled with the photosensitive cationic dye as a new nanocarrier for therapy and cellular imaging. Dyes Pigm. 2019, 161, 161-166 link
Sobotta, L., Ziental, D., Sniechowska, J., Dlugaszewska, J., Potrzebowski, M.J.. Lipid vesicle-loaded meso-substituted chlorins of high in vitro antimicrobial photodynamic activity. Photochem. Photobiol. Sci. 2019, 18, 213-223 link
Sobotta, L., Sniechowska, J., Ziental, D., Dlugaszewska, J., Potrzebowski, M.J. Chlorins with (trifluoromethyl)phenyl substituents – Synthesis, lipid formulation and photodynamic activity against bacteria. Dyes Pigm. 2019, 160, 292-300 link
Venâncio, T., Oliveira, L.M., Pawlak, T., Ellena, J., Boechat, N., Brown, S.P. The use of variable temperature 13C solid-state MAS NMR and GIPAW DFT calculations to explore the dynamics of diethylcarbamazine citrate. Magn. Reson. Chem. 2019, 57, 200–210 link
2018
Paluch, P., Pawlak, T., Lławniczak, K., Trébosc, J., Lafon, O., Amoureux, J.-P., Potrzebowski, M.J. Simple and Robust Study of Backbone Dynamics of Crystalline Proteins Employing 1 H– 15 N Dipolar Coupling Dispersion. J. Phys. Chem. B 2018, 122, 8146–8156. link
Dudek, M.K., Kostrzewa, M., Paluch, P., Potrzebowski, M.J. π-Philic molecular recognition in the solid state as a driving force for mechanochemical formation of apremilast solvates and cocrystals. Cryst. Growth Des. 2018, 18, 3959–3970. link
Wozniak, M., Michalak, B., Wyszomierska, J., Dudek, M.K., Kiss, A.K. Effects of phytochemically characterized extracts from Syringa vulgaris and isolated secoiridoids on mediators of inflammation in a human neutrophil model. Front. Phramacol. 2018, 9, 349(1-15) link
Lipiński, P.F.J., Garnuszek, P., Maurin, M., Stoll, R., Metzler-Nolte, N., Wodyński, A., Dobrowolski, J.C., Dudek, M.K., Orzełowska, M., Mikołajczak, R. Structural studies on radiopharmaceutical DOTA-minigastrin analogue (CP04) complexes and their interaction with CCK2 receptor. EJNMMI Research 2018, 8:33, 1-10 link
Adjiman, C.S., Brandenburg, J.G., Braun, D.E., Cole, J., Collins, C., Cooper, A.I., Cruz-Cabeza, A.J., Day, G.M., Dudek, M., Hare, A., Iuzzolino, L., McKay, D., Mitchell, J.B.O., Mohamed, S., Neelamraju, S., Neumann, M., Nilsson Lill, S., Nyman, J., Oganov, A.R., Price, S.L., Pulido, A., Reutzel-Edens, S., Rietveld, I., Ruggiero, M.T., Schön, J.C., Tsuzuki, S., van den Ende, J., Woollam, G., Zhu, Q. Applications of crystal structure prediction – organic molecular structures: general discussion. Faraday Discuss. 2018, 211, 493-539 link
Dudek, M.K., Kazmierski, S., Kostrzewa, M., Potrzebowski, M.J. Solid state NMR studies of molecular crystals. Annual Rep. NMR Spectrosc. 2018, 95, 1-81 link
Czerwińska, M.E., Dudek, M.K., Pawłowska, K.A., Pruś, A., Ziaja, M., Granica, S. The influence of procyanidins isolated from small-leaved lime flowers (Tilia cordata Mill.) on human neutrophils. Fitoterapia 2018, 127, 115–122 link
Śniechowska, J., Paluch, P., Pawlak, T., Bujacz, G.D., Danikiewicz, W., Potrzebowski, M.J. New synthetic pathway leading to oxospirochlorins. RSC Advances 2018, 8, 21354–21362 link
Łudzik, K., Kustrzepa, K., Kowalewicz-Kulbat, M., Kontek, R., Kontek, B., Wróblewska, A., Jóźwiak, M., Lulo, D. Antimicrobial and Cytotoxic Properties of Bisquaternary Ammonium Bromides of Different Spacer Length. J. Surfact. Deterg. 2018, 21, 91–99 link
Sowińska, A. Laskowska, A. Guspiel, J. Solecka, M. Bochynska-Czyż, A. W. Lipkowski, K. Trzeciak, Z. Urbańczyk-Lipkowska. Bioinspired Amphiphilic Peptide Dendrimers as Specific and Effective Compounds against Drug Resistant Clinical Isolates of E. coli. Bioconjugate Chem. 2018, 29, 3571–3585 link
Masnyk, M., Butkiewicz, A., Górecki, M., Luboradzki, R., Paluch, P., Potrzebowski, M.J., Frelek, J. In Depth Analysis of Chiroptical Properties of Enones Derived from Abietic Acid. J. Org. Chem. 2018, 83, 3547–3561 link
Głodek, M., Makal, A., Paluch, P., Kadziołka-Gaweł, M., Kobayashi, Y., Zakrzewski, J., Plazuk, D. (Ar–CO–CC)(PEt 3)Au and (Ar–CC)(PEt 3)Au Complexes Bearing Pyrenyl and Ferrocenyl Groups: Synthesis, Structure, and Luminescence Properties. Dalton Trans. 2018, 47, 6702–6712 link
2017
Wróblewska, A., Paluch, P., Wielgus, E., Bujacz, G., Dudek, M.K., Potrzebowski, M.J. Approach toward the understanding of coupling mechanism for EDC reagent in solvent free mechanosynthesis. Org. Lett. 2017, 19, 5360–5363 link
Dudek, M.K., Wielgus, E., Paluch, P., Potrzebowski, M.J. Spontaneous Keto–Enol Tautomerization in the Crystal Lattice Visualized with the Help of Water Encapsulated in Hydrophilic Reservoirs. ChemPhysChem 2017, 18, 2850-2854 link
Skorupska, E., Kaźmierski, S., Potrzebowski, M.J. Solid State NMR Characterization of Ibuprofen:Nicotinamide Cocrystals and New Idea for Controlling Release of Drugs Embedded into Mesoporous Silica Particles. Mol. Pharm. 2017, 14, 1800-1810 link
Miksa, B., Sierant, M., Skorupska, E., Michalski, A., Kazmierski, S., Steinke, U., Rozanski, A., Uznanski, P. Chlorambucil labelled with the phenosafranin scaffold as a new chemotherapeutic for imaging and cancer treatment. Colloids Surf. B Biointerfaces, 2017, 159, 820-828 link
Potrzebowski, M.J. Preface: Ultrafast magic-angle spinning NMR. Solid State Nucl. Magn. Reson. 2017, 87, 65-66 link
Dudek, M.K., Michalak, B., Woźniak, M., Czerwińska, M.E., Filipek, A., Granica, S., Kiss, A.K. Hydroxycinnamoyl derivatives and secoiridoid glycoside derivatives from Syringa vulgaris flowers and their effects on the pro-inflammatory responses of human neutrophils. Fitoterapia, 2017, 121, 194-205 link
Paluch, P., Trébosc, J., Amoureux, J.-P., Potrzebowski, M.J. 1H-31P CPVC NMR method under Very Fast Magic Angle Spinning for analysis of dipolar interactions and dynamics processes in the crystalline phosphonium tetrafluoroborate salts. Solid State Nucl. Magn. Reson. 2017, 87, 96-103 link
Dudek, M.K., Bujacz, G., Potrzebowski, M.J. Experimental tests for quality validation of computationally predicted crystal structures – a case of a conformationally flexible procyanidin A2 dihydrate.CrystEngComm 2017, 19, 2903–2913 link
Dudek, M.K., Gliński, V.B., Davey, M.H., Sliva, D., Kaźmierski, S., Gliński, J.A. Trimeric and Tetrameric A-Type Procyanidins from Peanut Skins. J. Nat. Prod. 2017, 80, 415-426 link
Nagashima, H., Trébosc, J., Lafon, O., Pourpoint, F., Paluch, P., Potrzebowski, M.J., Amoureux, J.-P. Imaging the spatial distribution of radiofrequency field, sample and temperature in MAS NMR rotor. Solid State Nucl. Magn. Reson. 2017, 87, 137-142 link
Paluch, P., Potrzebowska, N., Ruppert, A.M., Potrzebowski, M.J. Application of 1H and 27Al magic angle spinning solid state NMR at 60 kHz for studies of Au and Au-Ni catalysts supported on boehmite/alumina. Solid State Nucl. Magn. Reson. 2017, 84, 111-117 link
Śniechowska, J., Paluch, P., Potrzebowski, M.J. Structure and dynamics processes in free-base chlorins controlled by chemical modifications of macroring and aryl groups in meso-positions. RSC Adv. 2017, 7, 24795-24805 link
2016
Dudek, M.K., Pawlak, T., Paluch, P., Jeziorna, A., Potrzebowski, M.J. A Multi-Technique Experimental and Computational Approach to Study the Dehydration Processes in the Crystals of Endomorphin Opioid Peptide Derivative. Cryst. Growth Des. 2016, 16, 5312-5322 link
Nishiyama, Y., Malon, M., Potrzebowski, M.J., Paluch, P., Amoureux, J.P. Accurate NMR determination of C-H or N-H distances for unlabeled molecules. Solid State Nucl. Magn. Reson. 2016, 73, 15-21 link
Śniechowska, J., Paluch, P., Bujacz, G., Górecki, M., Frelek, J., Gryko, D.T., Potrzebowski, M.J. Chiral crystals from porphyrinoids possessing a very low racemization barrier. CrystEngComm 2016, 18, 3561-3565 link
Jastrzebska, I., Pawlak, T., Arcos-Ramos, R., Florez-Lopez, E., Farfán, N., Czajkowska-Szczykowska, D., Maj, J., Santillan, R., Morzycki, J.W., Potrzebowski, M.J. Synthesis, Structure, and Local Molecular Dynamics for Crystalline Rotors Based on Hecogenin/Botogenin Steroidal Frameworks. Cryst. Growth Des. 2016, 16, 5698-5709 link
Skorupska, E., Jeziorna, A., Potrzebowski, M.J. Thermal Solvent-Free Method of Loading of Pharmaceutical Cocrystals into the Pores of Silica Particles: A Case of Naproxen/Picolinamide Cocrystal. J. Phys. Chem. C 2016, 120, 13169-13180 link
Kaczmarek, R., Kaźmierski, S., Pawlak, T., Radzikowska, E., Baraniak, J. Assignment of the absolute configuration at stereogenic phosphorus atoms in P-diastereomers of dithymidyl-(N3′→P5′)-phosphoramidothioate. Tetrahedron 2016, 72, 803-809 link
Kaźmierski, S., Pawlak, T., Jeziorna, A., Potrzebowski, M.J. Modern solid state NMR techniques and concepts in structural studies of synthetic polymers. Polym. Adv. Technol. 2016, 27, 1143-1155 link
Granica, S., Kłȩbowska, A., Kosiński, M., Piwowarski, J.P., Dudek, M.K., Kaźmierski, S., Kiss, A.K. Effects of Geum urbanum L. root extracts and its constituents on polymorphonuclear leucocytes functions. Significance in periodontal diseases. J. Ethnopharmacol. 2016, 188, 1-12 link
Rode, J.E., Narbutt, J., Dudek, M.K., Kaźmierski, S., Dobrowolski, J.C. On the conformation of the actinide-selective hydrophilic SO3-Ph-BTP ligand in aqueous solution. A computational study. J. Mol. Liq. 2016, 219, 224-231 link
Dudek, M.K., Dudkowski, ., Bazylko, A., Kaźmierski, S., Kiss, A.K. Caffeic acid derivatives isolated from the aerial parts of Galinsoga parviflora and their effect on inhibiting oxidative burst in human neutrophils. Phytochem. Lett. 2016, 16, 303-310 link
Dudek, M.K., Jeziorna, A., Potrzebowski, M.J. Computational and experimental study of reversible hydration/dehydration processes in molecular crystals of natural products-a case of catechin. CrystEngComm 2016, 18, 5267-5277 link
2015
Wielgus, E., Paluch, P., Frelek, J., Szczepek, W.J., Potrzebowski, M.J. Full Characterization of Linezolid and Its Synthetic Precursors by Solid-State Nuclear Magnetic Resonance Spectroscopy and Mass Spectrometry. J. Pharm. Sci. 2015, 104, 3883-3892 link
Paluch, P., Pawlak, T., Jeziorna, A., Trébosc, J., Hou, G., Vega, A.J., Amoureux, J.-P., Dracinsky, M., Polenova, T., Potrzebowski, M.J. Analysis of local molecular motions of aromatic sidechains in proteins by 2D and 3D fast MAS NMR spectroscopy and quantum mechanical calculations. Phys. Chem. Chem. Phys. 2015, 17, 28789-28801 link
Skorupska, E., Paluch, P., Jeziorna, A., Potrzebowski, M.J. NMR study of BA/FBA cocrystal confined within mesoporous silica nanoparticles employing thermal solid phase transformation. J. Phys. Chem. C 2015, 119, 8652-8661 link
Sierant, M., Kazmierski, S., Rozanski, A., Paluch, P., Bienias, U., Miksa, B.J. Nanocapsules for 5-fluorouracil delivery decorated with a poly(2-ethylhexyl methacrylate-co-7-(4-trifluoromethyl)coumarin acrylamide) cross-linked wall. New J. Chem. 2015, 39, 1506-1516 link
Paluch, P., Pawlak, T., Oszajca, M., Lasocha, W., Potrzebowski, M.J. Fine refinement of solid state structure of racemic form of phospho-tyrosine employing NMR Crystallography approach. Solid State Nucl. Magn. Reson. 2015, 65, 2-11 link
Jeziorna, A., Stopczyk, K., Skorupska, E., Luberda-Durnas, K., Oszajca, M., Lasocha, W., Górecki, M., Frelek, J., Potrzebowski, M.J. Cyclic dipeptides as building units of nano- and microdevices: Synthesis, properties, and structural studies. Cryst. Growth Des. 2015, 15, 5138-5148 link
Paluch, P., Trébosc, J., Nishiyama, Y., Potrzebowski, M.J., Malon, M., Amoureux, J.P. Theoretical study of CP-VC: A simple, robust and accurate MAS NMR method for analysis of dipolar C-H interactions under rotation speeds faster than ca. 60 kHz. J. Magn. Reson. 2015, 252, 67-77 link
Masalski, J., Wawrzaszek, U., Potrzebowski, M.J., Kucharczyk, B., Chęcmanowski, J.G., Tylus, W., Szczygieł, B. Solid state NMR and EIS examination of SiO<inf>2</inf>-epoxy hybrid coatings on stainless steel. Solid State Phenom. 2015, 227, 131-134 link
Pawlak, T., Kowalewska, A., Zgardzińska, B., Potrzebowski, M.J. Structure, Dynamics, and Host-Guest Interactions in POSS Functionalized Cross-Linked Nanoporous Hybrid Organic-Inorganic Polymers. J. Phys. Chem. C 2015, 119, 26575-26587 link
Vícha, J., Foroutan-Nejad, C., Pawlak, T., Munzarová, M.L., Straka, M., Marek, R. Understanding the electronic factors responsible for ligand spin-orbit NMR shielding in transition-metal complexes. J. Chem. Theor. Comput. 2015, 11, 1509-1517 link
Niedzielska, D., Pawlak, T., Wojtczak, A., Pazderski, L., Szlyk, E. Structural and 1H, 13C, 15N NMR spectroscopic studies of Pd(II) chloride organometallics with 2-phenylpyridine and ammonia, pyridine or its methyl derivatives. Polyhedron 2015, 92, 41-51 link
Miksa, B. Recent progress in designing shell cross-linked polymer capsules for drug delivery. RSC Adv. 2015, 5, 87781-87805 link
selected older papers from 2000 – 2014
2014
Bocian, W., Paluch, P., Nowak-Król, A., Gryko, D.T., Potrzebowski, M., Sniechowska, J., Sitkowski, J., Bednarek, E., Kozerski, L. The 1H, 13C, 15N, and 19F NMR chemical shifts assignments in 5,10,15-tris (pentafluorophenyl) tetra- 15 N corrole at 191 K. Magn. Reson. Chem. 2014, 53, 167-171
Huben, K., Jewgiński, M., Pabis, A., Paluch, P., Luy, B., Jankowski, S. The structure of cyclolinopeptide a in chloroform refined by RDC measurements. J. Pept. Sci. 2014, 20, 901-907
Skorupska, E., Jeziorna, A., Paluch, P., Potrzebowski, M.J. Ibuprofen in mesopores of mobil crystalline material 41 (MCM-41): A deeper understanding. Mol. Pharm. 2014, 11, 1512-1519
Szymański, S., Paluch, P., Gryko, D.T., Nowak-Król, A., Bocian, W., Sitkowski, J., Koszarna, B., Śniechowska, J., Potrzebowski, M.J., Kozerski, L. Insights into the tautomerism in meso-substituted corroles: A variable-temperature 1H, 13C, 15N, and 19F NMR spectroscopy study. Chem. Eur. J. 2014, 20, 1720-1730
Jeziorna, A., Kazmierski, S., Paluch, P., Skorupska, E., Potrzebowski, M.J. Recent progress in the solid-state NMR studies of short peptides. techniques, structure and dynamics. Annual Rep. NMR Spectr. 2014, 83, 67-143
Pawlak, T., Paluch, P., Jeziorna, A., Bujacz, G.D., Potrzebowski, M.J. Slow and very fast MAS solid state NMR study of biopolymers. Macromol. Symp. 2014, 339, 60-69
Pawlak, T., Niedzielska, D., Vícha, J., Marek, R., Pazderski, L. Dimeric Pd(II) and Pt(II) chloride organometallics with 2-phenylpyridine and their solvolysis in dimethylsulfoxide. J. Organometal. Chem. 2014, 759, 58-66 Pawlak, T., Potrzebowski, M.J. Fine refinement of solid-state molecular structures of Leu- and met-enkephalins by NMR crystallography. J. Phys. Chem. B 2014, 118, 3298-3309
Skorupska, E., Jeziorna, A., Kazmierski, S., Potrzebowski, M.J. Recent progress in solid-state NMR studies of drugs confined within drug delivery systems. Solid State Nucl. Magn. Reson. 2014, 57-58, 2-16
Szubert, K., Marciniec, B., Dutkiewicz, M., Potrzebowski, M.J., Maciejewski, H. Functionalization of spherosilicates via hydrosilylation catalyzed by well-defined rhodium siloxide complexes immobilized on silica. J. Mol. Catal. A Chem. 2014, 391, 150-157
2013
Kobayashi, T., Mao, K., Paluch, P., Nowak-Krõl, A., Sniechowska, J., Nishiyama, Y., Gryko, D.T., Potrzebowski, M.J., Pruski, M. Study of intermolecular interactions in the corrole matrix by solid-state NMR under 100 kHz MAS and theoretical calculations. Angew. Chem Int. Ed. 2013, 52, 14108-14111
Pawlak, T., Paluch, P., Trzeciak-Karlikowska, K., Jeziorna, A., Potrzebowski, M.J. Study of the thermal processes in molecular crystals of peptides by means of NMR crystallography. CrystEngComm 2013, 15, 8680-8692
Paluch, P., Kaźmierski, S., Jeziorna, A., Sniechowska, J., Dabrowa, K., Panek, J.J., Jezierska-Mazzarello, A., Jurczak, J., Potrzebowski, M.J. Influence of environmental humidity on organization and molecular dynamics of heteromacrocyclic assemblies. J. Phys. Chem. B 2013, 117, 14420-14431
Sierant, M., Paluch, P., Florczak, M., Rozanski, A., Miksa, B. Photosensitive nanocapsules for use in imaging from poly(styrene-co-divinylbenzene) cross-linked with coumarin derivatives. Colloids Surf. B Biointerfaces 2013, 111, 571-578
Drabik, E., Jeziorna, A., Bienias, U., Trzeciak-Karlikowska, K., Pawlak, T., Paluch, P., Potrzebowski, M.J. Study of the mechanism of thermal chemical processes in the crystals of YAF tripeptides by means of mass spectrometry and solid state NMR. J. Phys. Chem. B 2013, 117, 13481-13489
Ghorbanloo, M., Jaworska, M., Paluch, P., Li, G.-D., Zhou, L.-J. Synthesis, characterization, and catalytic activity for thioanisole oxidation of homogeneous and heterogeneous binuclear manganese(II) complexes with amino acid-based ligands. Transit. Metal Chem. 2013, 38, 511-521
Deredas, D., Albrecht, Ł., Maniukiewicz, W., Wojciechowski, J., Wolf, W.M., Paluch, P., Janecki, T., Rózalski, M., Krajewska, U., Janecka, A., Krawczyk, H. Three-component reaction of 3-(diethoxyphosphoryl)coumarin, enolizable ketones and primary amines: Simple, stereoselective synthesis of benzo[1,3]oxazocine skeletons. RSC Advances 2013, 3, 6821-6832
Midura, W.H., Sobczak, A., Paluch, P. Stereoselective cyclopropyl phosphonate formation using (S)-dimethylsulfonium-(p-tolylsulfinyl)methylide. Unusual phosphoryl group migration. Tetrahedron Lett. 2013, 54, 223-226
Paluch, P., Pawlak, T., Amoureux, J.-P., Potrzebowski, M.J. Simple and accurate determination of X-H distances under ultra-fast MAS NMR. J. Magn. Reson. 2013, 233, 56-63
Niedzielska, D., Pawlak, T., Czubachowski, T., Pazderski, L. 1H, 13C, and 15N NMR studies of Au(III) and Pd(II) chloride complexes and organometallics with 2-acetylpyridine and 2-benzoylpyridine. J. Spectrosc. 2013, 1, art. no. 982832
Pawlak, T., Jaworska, M., Potrzebowski, M.J. NMR crystallography of α-poly(L-lactide). Phys. Chem. Chem. Phys. 2013, 15, 3137-3145
Niedzielska, D., Pawlak, T., Bozejewicz, M., Wojtczak, A., Pazderski, L., Szlyk, E. Structural and spectroscopic studies of Au(III) and Pd(II) chloride complexes and organometallics with 2-benzylpyridine. J. Mol. Struct. 2013, 1032, 195-202
Czernek, J., Pawlak, T., Potrzebowski, M.J., Brus, J. The comparison of approaches to the solid-state NMR-based structural refinement of vitamin B1 hydrochloride and of its monohydrate. Chem. Phys. Lett. 2013, 555, 135-140
Miksa, B.J., Sochacki, M., Sroka-Bartnicka, A., Uznański, P., Nosal, A., Potrzebowski, M.J. Application of parylene for surface (polymer) enhanced laser desorption/ionization of synthetic polymers. Rapid Commun. Mass Spectr. 2013, 27, 767-772
2012
Jeziorna, A., Pawlak, T., Trzeciak-Karlikowska, K., Paluch, P., Potrzebowski, M.J. Magic angle spinning NMR study of interaction of N-terminal sequence of dermorphin (Tyr-d-Ala-Phe-Gly) with phospholipids. Biochim. Biophys. Acta Biomembr. 2012, 1818, 2579-2587
Walczak, M., Ciesielski, W., Galeski, A., Potrzebowski, M.J., Regnier, G., Hiltner, A., Baer, E. Structure and molecular dynamics of multilayered polycarbonate/polystyrene films. J. Appl. Polym Sci. 2012, 125, 4267-4274
Jaworska, M., Jeziorna, A., Drabik, E., Potrzebowski, M.J. Solid state NMR study of thermal processes in nanoassemblies formed by dipeptides. J. Phys. Chem. C 2012, 116, 12330-12338
Miksa, B., Sochacki, M., Libiszowski, J., Duda, A., Ciesielski, W., Potrzebowski, M.J. Application of ionic liquid matrices in spectral analysis of poly(lactide) – Solid state NMR spectroscopy versus matrix-assisted laser desorption/ ionization time-of-flight (MALDI-TOF) mass spectrometry. Anal. Methods 2012, 4, 377-383
Jaworska, M., Pawlak, T., Kruszyński, R., Ćwiklińska, M., Krzemiński, M. NMR crystallography comparative studies of chiral (1 R,2 S,3 R,5 R)-3-amino-6,6-dimethylbicyclo[3.1.1]heptan-2-ol and its p-toluenesulfonamide derivative. Cryst. Growth Des. 2012, 12, 5956-5965
Czernek, J., Pawlak, T., Potrzebowski, M.J. Benchmarks for the 13C NMR chemical shielding tensors in peptides in the solid state. Chem. Phys. Lett. 2012, 527, 31-35
Pawlak, T., Trzeciak-Karlikowska, K., Czernek, J., Ciesielski, W., Potrzebowski, M.J. Computed and experimental chemical shift parameters for rigid and flexible YAF peptides in the solid state. J. Phys. Chem. B 2012, 116, 1974-1983
2011
Nowicka, K., Bujacz, A., Paluch, P., Sobczuk, A., Jeziorna, A., Ciesielski, W., Bujacz, G.D., Jurczak, J., Potrzebowski, M.J. Study of host-guest interactions in benzodiazacoronands by means of solid state NMR spectroscopy, X-ray diffraction and quantum mechanical computations. Phys. Chem. Chem. Phys. 2011, 13, 6423-6433
Pawlak, T., Munzarová, M.L., Pazderski, L., Marek, R. Validation of relativistic DFT approaches to the calculation of NMR chemical shifts in square-planar Pt2+ and Au3+ complexes. J. Chem. Theor. Comput. 2011, 7, 3909-3923
Trzeciak-Karlikowska, K., Bujacz, A., Ciesielski, W., Bujacz, G.D., Potrzebowski, M.J. The influence of the stereochemistry of alanine residue on the solid state conformation and crystal packing of opioid peptides containing D-Ala or L-Ala in message domain – XRD and NMR study. J. Phys. Chem. B 2011, 115, 9910-9919
Marciniec, B., Rogalski, S., Potrzebowski, M.J., Pietraszuk, C. Ruthenium Carbene Siloxide Complexes Immobilized on Silica: Synthesis and Catalytic Activity in Olefin Metathesis. ChemCatChem 2011, 3, 904-910Ciesielski, W., Kassassir, H., Potrzebowski, M.J. A practical guide for the setup of a 1H- 31P- 13C double cross-polarization (DCP) experiment. Solid State Nucl. Magn. Reson. 2011, 39, 151-157
2010
Jaworska, M., Hrynczyszyn, P.B., Wełniak, M., Wojtczak, A., Nowicka, K., Krasiński, G., Kassassir, H., Ciesielski, W., Potrzebowski, M.J. Solid state NMR spectroscopy as a precise tool for assigning the tautomeric form and proton position in the intramolecular bridges of o-hydroxy schiff bases. J. Phys. Chem. A 2010, 114, 12522-12530
Potrzebowski, M.J., Kaźmierski, S., Kassassir, H., Miksa, B. Phosphorus-31 NMR Spectroscopy of Condensed Matter. Annual Rep. NMR Spectrosc. 2010, 70, 35-114
Sroka-Bartnlcka, A., Ciesielski, W., Libiszowski, J., Duda, A., Sochacki, M., Potrzebowski, M.J. Complementarity of solvent-free MALDI TOF and solid-state NMR spectroscopy in spectral analysis of polylactides. Anal. Chem. 2010, 82, 323-328
2009
Paluch, P., Potrzebowski, M.J. Combined solid state NMR and ONIOM studies of reversible crystalline phase reaction for nickel coordination compounds. Solid State Nucl. Magn. Reson. 2009, 36, 103-109
Marciniec, B., Szubert, K., Potrzebowski, M.J., Kownacki, I., Maciejewski, H. Catalysis of hydrosilylation by well-defined surface rhodium siloxide phosphine complexes. ChemCatChem 2009, 1, 304-310
Trzeciak-Karlikowska, K., Bujacz, A., Jeziorna, A., Ciesielski, W., Bujacz, G.D., Gajda, J., Pentak, D., Potrzebowski, M.J. Solid-state NMR and X-ray diffraction study of structure and dynamics of dihydrate and anhydrous form of Tyr-Ala-Phe. Cryst. Growth Des. 2009, 9, 4051-4059
Marciniec, B., Szubert, K., Fiedorow, R., Kownacki, I., Potrzebowski, M.J., Dutkiewicz, M., Franczyk, A. Catalysis of hydrosilylation by well-defined rhodium siloxide complexes immobilized on silica. J. Mol. Cat. A Chem. 2009, 310, 9-16
Sroka-Bartnicka, A., Olejniczak, S., Ciesielski, W., Nosal, A., Szymanowski, H., Gazicki-Lipman, M., Potrzebowski, M.J. Solid state NMR study and density functional theory (DFT) calculations of structure and dynamics of poly(p-xylylenes). J. Phys. Chem. B 2009, 113, 5464-5472
Sroka-Bartnicka, A., Olejniczak, S., Sochacki, M., Biela, T., Potrzebowski, M.J. Solid-State NMR Spectroscopy as a Tool Supporting Optimization of MALDI-TOF MS Analysis of Polylactides. J. Am. Soc. Mass Spec. 2009, 20, 67-72
2008
Gajda, J., Olejniczak, S., Bryndal, I., Potrzebowski, M.J. Elucidation of structural restraints for phosphate residues with different hydrogen bonding and ionization states. J. Phys. Chem. B 2008, 112, 14036-14044
Potrzebowski, M.J., Potrzebowski, W.M., Jeziorna, A., Ciesielski, W., Gajda, J., Bujacz, G.D., Chruszcz, M., Minor, W. Synthesis and solid-state study of supramolecular host-guest assemblies: Bis[6-O,6-O′-(1,2:3,4-diisopropylidene-α-D-galactopyranosyl) thiophosphoryl] dichalcogenides. J. Org. Chem. 2008, 73, 4388-4397Potrzebowski, M.J., Jeziorna, A., Kaźmierski, S. NMR studies of chiral organic compounds in non-isotropic phases. Concepts Magn. Reson. Part A Bridg. Educ. Res. 2008, 32, 201-218
Gajda, J., Potrzebowski, M.J., Bujacz, A., Bujacz, G. Application of the 77Se solid state NMR for investigation of bioorganic compounds – the case of selenomethionine. Phosphorus Sulfur Silicon Relat. Elem. 2008, 183, 1061-1066
Marciniec, B., Szubert, K., Potrzebowski, M.J., Kownacki, I., Łȩszczak, K. Synthesis, characterization, and catalytic activity of a well-defined rhodium siloxide complex immobilized on silica. Angew. Chem. Int. Ed. 2008, 47, 541-544
Olejniczak, S., Mikuła-Pacholczyk, J., Hughes, C.E., Potrzebowski, M.J. 15N and 13C high-resolution solid-state NMR study of the polymorphism of the L-enantiomer of N-benzoylphenylalanine. J. Phys. Chem. B 2008, 112, 1586-1593
2007
Dołega, A., Baranowska, K., Gajda, J., Kaźmierski, S., Potrzebowski, M.J. Cadmium tri-tert-butoxysilanethio-lates: Structural and spectroscopic models of metal sites in proteins. Inorg. Chim. Acta 2007, 360, 2973-2982
Gajda, J., Jeziorna, A., Ciesielski, W., Potrzebowski, W.M., Prezdo, W.W., Potrzebowski, M.J. High-resolution solid-state NMR spectroscopy as a tool for investigation of enantioselective inclusion complexation. Solid State Nucl. Magn. Reson. 2007, 31, 153-161
Pacholczyk, J., Kalisiak, J., Jurczak, J., Potrzebowski, M.J. Search of nature of planar chirality for pendent benzodiazacoronands in the solid state: NMR, X-ray, and DFT studies. J. Phys. Chem. B 2007, 111, 2790-2799
2006
Gajda, J., Pacholczyk, J., Bujacz, A., Bartoszak-Adamska, E., Bujacz, G., Ciesielski, W., Potrzebowski, M.J. Structure and dynamics of L-selenomethionine in the solid state. J. Phys. Chem. B 2006, 110, 25692-25701
Olejniczak, S., Napora, P., Gajda, J., Ciesielski, W., Potrzebowski, M.J. 31P double-quantum solid-state NMR study of phosphoroorganic compounds with (O)P-O-P-(O), (S)P-O-P(S) and (S)P-S-P(O) unit. Solid State Nucl. Magn. Reson. 2006, 30, 141-149
Potrzebowski, M.J., Ciesielski, W., Ganicz, K., Głuszek, J., Szczygiel, B., Kucharczyk, B., Masalski, J. 29Si and 13C solid state NMR as a tool to study thermal processes in epoxy-silica hybrids. Pol. J. Chem. 2006, 80, 1185-1194
Potrzebowski, M.J., Gajda, J., Ciesielski, W., Montesinos, I.M. Distance measurements in disodium ATP hydrates by means of 31P double quantum two-dimensional solid-state NMR spectroscopy. J. Magn. Reson. 2006, 179, 173-181
Kurdziel, K., Olejniczak, S., Okruszek, A., Głowiak, T., Kruszyński, R., Materazzi, S., Potrzebowski, M.J. Search of structure and ligands exchange for palladium(II) complexes with N-allylimidazole; X-ray and solid-state/solution NMR studies. J. Organometal. Chem. 2006, 691, 869-878
Potrzebowski, M.J., Bujacz, G.D., Bujacz, A., Olejniczak, S., Napora, P., Heliński, J., Ciesielski, W., Gajda, J. Study of molecular dynamics and the solid state phase transition mechanism for unsymmetrical thiopyrophosphate using X-ray diffraction, DFT calculations and NMR spectroscopy. J. Phys. Chem. B 2006, 110, 761-771
Potrzebowski, M.J., Heliński, J., Olejniczak, S., Ciesielski, W. Understanding self-organization of the inclusion complexes in the solid state – DSC, NMR and DFT studies. J. Phys. Org. Chem. 2006, 19, 53-60
2005
Hughes, C.E., Olejniczak, S., Helinski, J., Ciesielski, W., Repisky, M., Andronesi, O.C., Potrzebowski, M.J., Baldus, M. Probing structure in the polymorphic domain of the L-enantiomer of N-benzoyl-phenylalanine by means of 2D solid-state NMR spectroscopy and DFT calculations. J. Phys. Chem. B 2005, 109, 23175-23182
Potrzebowski, M.J., Kaźmierski, S., Olejniczak, S., Heliński, J., Ciesielski, W., Dolle, A. Comparative analysis of NMR spectral parameters and molecular dynamics of 1:6-anhydro-3:4-thia-2-O-tosyl-βD-allopyranose and 1,6:3,4-dianhydro-2-O- tosyl-β-D-galactopyranose in the solid phase. J. Phys. Org. Chem. 2005, 18, 602-609
Michalski, J., Kucharska, E., Wandas, M., Hanuza, J., Waśkowska, A., Ma̧czka, M., Talik, Z., Olejniczak, S., Potrzebowski, M.J. Crystal structure, vibrational and NMR studies and chemical quantum calculations of 2-phenylazo-5-nitro-6-methyl-pyridine (C12H 10N4O2). J. Mol. Struct. 2005, 744-747, 377-392
2004
Olejniczak, S., Potrzebowski, M.J. Solid state NMR studies and density functional theory (DFT) calculations of conformers of quercetin. Org. Biomol. Chem. 2004, 2, 2315-2322
Olejniczak, S., Potrzebowski, M.J., Wozniak, L.A. Synthesis and NMR structural analysis of 2κ-OMe-Uridin-3′-yl (3′,5′)-5′-O-(N-isobutyryl-2′-OMe-cytidine) methylthiophosphonates. Eur. J. Org. Chem. 2004, 9, 1958-1966
Olejniczak, S., Sobczak, M., Potrzebowski, M.J., Polak, M., Plavec, J., Nawrot, B. Assignment of absolute configuration at phosphorus of P-chiral diastereomers of deoxyribonucleoside methanephosphonamidates by means of NMR spectroscopy. Tetrahedron 2004, 60, 3979-3986
Słabicki, M.M., Potrzebowski, M.J., Bujacz, G., Olejniczak, S., Olczak, J. X-ray and Nuclear Magnetic Resonance (NMR) Studies of Signalizing the Tripeptide Sequence (Tyr-D-Ala-Phe) of Dermorphin and Deltorphins I and II. Comparative Analysis in the Liquid and Solid Phases. J. Phys. Chem. B 2004, 108, 4535-4545
Wang, F., Polavarapu, P.L., Drabowicz, J., Kiełbasinski, P., Potrzebowski, M.J., Mikołajczyk, M., Wieczorek, M.W., Majzner, W.W., Łazewska, I. Solution and crystal structures of chiral molecules can be significantly different: Tert-butylphenylphosphinoselenoic acid. J. Phys. Chem. A 2004, 108, 2072-2079
2003
Grossmann, G., Potrzebowski, M.J., Olejniczak, S., Ziółkowska, N.E., Bujacz, G.D., Ciesielski, W., Prezdo, W., Nazarov, V., Golovko, V. Structural studies of N-(2′-substituted phenyl)-9,10-dihydro-9,10-ethanoanthracene-11,12-dicarboximides by X-ray diffraction and NMR spectroscopy – Proofs for CH/π interactions in liquid and solid phases. New J. Chem. 2003, 27, 1095-1101
Potrzebowski, M.J., Assfeld, X., Ganicz, K., Olejniczak, S., Cartier, A., Gardiennet, C., Tekely, P. An experimental and theoretical study of the 13C and 31P chemical shielding tensors in solid O-phosphorylated amino acids. J. Am. Chem. Soc. 2003, 125, 4223-4232
Potrzebowski, M.J. What high-resolution solid-state NMR spectroscopy can offer to organic chemists. Eur. J. Org. Chem. 2003, 8, 1367-1376
2002
Potrzebowski, M.J., Tadeusiak, E., Misiura, K., Ciesielski, W., Bujacz, G., Tekely, P. A new method for distinguishing between enantiomers and racemates and assignment of enantiomeric purity by means of solid-state NMR. Examples from oxazaphosphorinanes. Chem. Eur. J. 2002, 8, 5007-5011
Potrzebowski, M.J., Grossmann, G., Ganicz, K., Olejniczak, S., Ciesielski, W., Kozioł, A.E., Wawrzycka, I., Bujacz, G., Haeberlen, U., Schmitt, H. X-ray, 31P CP/MAS, and single-crystal NMR studies, and 31P DFT GIAO calculations of inclusion complexes of Bis[6-o,6-o′-(1,2:3,4-diisopropylidene-α-D-galactopyranosyl) thiophosphoryl] disulfide: The importance of C-H···S=P contacts in the solid state. Chem. Eur. J. 2002, 8, 2691-2699
Tekely, P., Gardiennet, C., Potrzebowski, M.J., Sebald, A., Reichert, D., Luz, Z. Probing molecular geometry of solids by nuclear magnetic resonance spin exchange at the n=0 rotational-resonance condition. J. Chem. Phys. 2002, 116, 7607-7616
Smolarz, H.D., Potrzebowski, M.J. Persilben, a new carboxystilbene from Polygonum persicaria. J. Mol. Struct. 2002, 605, 151-156
Molchanov, S., Orzelski, W., Gryff-Keller, A., Potrzebowski, M.J. Magnetic shielding tensors of carbon nuclei in 3,5-dichlorophenylacetylene, a theoretical ab initio and experimental study. Mol. Phys. 2002, 100, 273-286
Potrzebowski, M.J., Helinski, J., Ciesielski, W. Two-dimensional and variable temperature 31P solid-state NMR studies of single crystals containing symmetrical/unsymmetrical bis[6-O,6-O′-(1,2:3,4-diisopropylidene-α-D-galactopyranosyl)thiophosphoryl] dichalcogenides. Chem. Commun. 2002, 2, 1582-1583.
2001
Potrzebowski, M.J., Ganicz, K., Kaźmierski, S. 31P high resolution solid state NMR studies of phosphoroorganic compounds of biological interest. Polish Journal of Chemistry 2001, 75, 1147-1169
Potrzebowski, M.J., Kaźmierski, S., Michalska, M., Olejniczak, S., Ciesielski, W., Latanowicz, L. Investigation of structure and motional behavior of 1,6:3,4-dianhydro-2-O-tosyl-β-D-galactopyranose in solution by means of multiple-field NMR spectroscopy. J. Mol. Struct. 2001, 597, 7-19
Potrzebowski, M.J., Yang, X.-B., Misiura, K., Majzner, W.R., Wieczorek, M.W., Kaźmierski, S., Olejniczak, S., Stec, W.J. Synthesis and structural studies of SP and RP diastereomers of deoxyxylothymidyl-3′-O-acetylthymidyl (3′,5′)-O(2-Cyanoethyl)phosphorothioate in solution and in the solid state. Eur. J. Org. Chem. 2001, 8, 1491-1501
2000
Potrzebowski, M.J., Tekely, P., Bandłaszczyk, J., Wieczorek, M.W. X-ray and 13C solid-state NMR studies of N-benzoylphenylalanine. J. Pept. Res. 2000, 56, 185-194
Kamierski, S., Olejniczak, S., Potrzebowski, M.J. 13C high-resolution solid state NMR studies of the structure and dynamics of 1,6:3,4-dianhydro-2-O-tosyl-β-d-galactopyranose. Solid State Nucl. Magn. Reson. 2000, 16, 131-139
Yang, X.-B., Misiura, K., Stec, W.J., Potrzebowski, M.J., Kazmierski, S., Wieczorek, M., Majzner, W.R., Bujacz, G.D. Nucleophilic N1→N3 rearrangement of 5′-O-trityl-O2,3′-cycloanhydrothymidine. Nucleosides Nucleotides Nucleic Acids 2000, 19 , 1657-1673
